TECHNOLOGIES

Modeling of Densification Kinetics during Electro-Pulse Consolidation of Titanium Powder

  • 1 Institute of Pulse Processes and Technologies of NAS of Ukraine, Bohoyavlenskyi ave., 43-A, 54018, Mykolaiv, Ukraine

Abstract

This study presents a theoretical investigation of the densification kinetics of titanium powder during electro-pulse consolidation. A mathematical model was developed to analyze the influence of electrical current parameters in different sintering regimes – direct current (DC), alternating current (AC), pulsed current, and their superposition – on the thermophysical processes governing sintering.
The heating rates and the evolution of relative density were calculated for different applied pressing pressures. The results show that the superposition of currents is the most energy-efficient regime. This regime enables the material to reach a relative density above 99% within a minimal processing time. The effect is attributed to the combined action of intense Joule heating and the electroplastic effect.

Keywords

References

  1. Spark Plasma Sintering Systems. Dr. Sinter Lab Series : product catalog / SPS Syntex Inc. – Kawasaki, Japan, 2023. – 12 p.
  2. Field Assisted Sintering Technology (FAST) / Spark Plasma Sintering (SPS) : systems specification / FCT Systeme GmbH. – Rauenstein, Germany, 2022. – 8 p.
  3. Gleeble 3800 Physical Simulation System : user guide / Dynamic Systems Inc. – Poestenkill, NY, USA, 2019. – 45 p.
  4. O. Syzonenko, M. Prystash, A. Zaichenko, O. Kovalenko, Materials Science. Non-Equilibrium Phase Transformations. 4(2), 41–44 (2018).
  5. Halliday, D., Resnick, R., & Walker, J. (2013). Fundamentals of Physics. 10th Edition. Wiley.
  6. Olevsky, E. A. (1998). Theory of sintering: from particular models to continuum theory. Materials Science and Engineering: R: Reports, 23(2), 41-100. (У статті розглядаються різні моделі для ефективних властивостей пористих тіл).
  7. Nilsson, J. W., & Riedel, S. A. (2015). Electric Circuits. 10th Edition. Pearson.
  8. Incropera, F. P., DeWitt, D. P., Bergman, T. L., & Lavine, A. S. (2007). Fundamentals of Heat and Mass Transfer. 6th Edition. Wiley.
  9. German, R. M. (2014). Sintering: From Empirical Observations to Scientific Principles. 2nd Edition. Butterworth-Heinemann.
  10. Atkins, P., & de Paula, J. (2014). Atkins' Physical Chemistry. 10th Edition. Oxford University Press.
  11. Orrù, R., Licheri, R., Locci, A. M., Cincotti, A., & Cao, G. (2009). Consolidation/synthesis of materials by electric current activated/assisted sintering. Materials Science and Engineering: R: Reports, 63(4-6), 127-287.
  12. ASM Handbook, Volume 2: Properties and Selection: Nonferrous Alloys and Special-Purpose Materials. (1990). ASM International.
  13. Incropera, F. P., DeWitt, D. P., Bergman, T. L., & Lavine, A. S. (2007). Fundamentals of Heat and Mass Transfer. 6th Edition. Wiley.
  14. Munir, Z. A., Anselmi-Tamburini, U., & Ohyanagi, M. (2006). The effect of electric field and pressure on the synthesis and consolidation of materials: A review of the spark plasma sintering method. Journal of Materials Science, 41(3), 763–777.
  15. Grasso, S., Sakka, Y., & Maizza, G. (2009). Electric current activated/assisted sintering (ECAS): a review of patents 1906–2008. Science and Technology of Advanced Materials, 10(5), 053001.

Article full text

Download PDF