International Scientific Journals
of Scientific Technical Union of Mechanical Engineering "Industry 4.0"

Electrochemical coatings of chromium modified with nanodiamond particles applied directly on niobium-aluminum alloy were obtained. Nanodiamond particles produced by detonation synthesis were used. Chromium coatings were deposited on a monolithic composite with a complex structure based on niobium and aluminum alloys, called later matrix for short. Standard chromium electrolyte and electrolyte with nanodiamond particles concentration of 10 g/l were used. Analyzes were performed by Scanning Electron Microscope system of Bruker Inc. and the Polyvar Met metallographic microscope. The microhardness was measured using a PolyvarMet 4000 microhardness tester. The obtained results of the microhardness were 788 kg/mm2 in the chromium layer and 168 kg/mm2 and 692 kg/mm2 in the matrix. The microstructural and SEM-EDS analysis showed the presence of two intermetallides Nb2Al and Nb3Al in the monolithic composite of niobium aluminum matrix. The average thickness of the chromium coatings modified with nanodiamond particles is 55 μm.

Heat-resistant composites with a layered niobium-based matrix reinforced with single-crystal sapphire fibers have been obtained. The fibers were grown from the melt by the modified Stepanov method. The composites were prepared by solid-phase technology by diffusion welding of multilayer packages of foils of the Nb–0.1% C and aluminum alloy, interlaid with sapphire fibers in layers of a suspension mixture of Nb powder. The production of fibers, their structure and strength testing procedure are described. The formation of multilayer packets, the structure and results of bending strength tests of composites are presented