International Scientific Journals
of Scientific Technical Union of Mechanical Engineering "Industry 4.0"

Silica gels are one of the most widely used adsorbents. The best view of the properties of silicas as catalytic supports, adsorbents and other applications give the adsorption-texture parameters and especially the specific surface area. Hydrated silicon dioxide is amorphous (SiO2.nH2O),a reactive compound with various contains. Due to the serious practical interest of the determination of the specific surface area of materials many methods are developed and have found application. The study evaluates the impact of the surface and surface modification on the possibility of an express method for determination of specific surface areas of silica gels.

The paper deals with the problem of occurrence of internal defects in materials produced by SLM technology. The influence of the position of materials on the platform during the SLM on selected properties – porosity and corrosion resistance were examined. The reuse of non-compacted powder (three times recycled powder) and its effect on porosity and corrosion resistance of materials was also tested. Porosity was measured on metallographic sections in two perpendicular directions by image analysis, corrosion properties were tested by linear polarization method.

The results of the estimation for the influence of titanium diboride content in the initial powder mixture on the basic mechanical properties at the tests on tension and compression are presented. It is shown that the porosity of sintered at 1250 0C preforms from TiH2-TiB2 powder mixture increases with increasing of titanium diboride content in the initial charge, which is due to the manifestation of the Frenkel effect at sintering. The values of tensile strength, hardness and elastic modulus, despite some porosity growth of the sintered alloy, increase with the addition of 5 % of TiB2 powder, while increasing the content of the high modulus component in the mixture to 10 % leads to decrease in the level of these characteristics. The plasticity of sintered alloys monotonically decreases with increasing of the boride component content. At compression tests, the yield point and the compressive strength increase monotonically with increase in TiB2 content, despite the increase in porosity of the latter, due to a significantly lower effect of porosity on the value of the resistance to deformation in compression compared with tension. The use of hot forging of sintered powder preforms leads to increase of strength properties and hardness of the composites.

The potential of using the ultrafine dispersion powder material obtained by the ECA pressing from a copper powder have considered for the production of fast-acting fuse links. The dependences of the density and microhardness along the length of the sample under different deformation conditions obtained. A deformation zone of constant density is determined and recommended for using in the production of fuse links. The dependence of the electrical resistance along the sample cross-section and across the deformation axis has determined. The fuse links calculation procedure has proposed.

Theoretical and experimental data on the impact of heating rate during spark-plasma sintering on densification kinetics, grain size and capillary pressure in powder compacts, based on Fe, are given. It is found out, that an increase of heating rate in range from 10 °C/s to 20 °C/s leads to acceleration of process of obtainment of non-porous compacts and decrease of structure grain size.